Preparation of fungal total RNA

Summary

Total RNA was extracted from a variety of different fungi.

Operation method

Preparation of fungal total RNA

Materials and Instruments

Phenol Chloroform Isoamyl alcohol 12mol L Lithium chloride 3mol L Sodium acetate Ethanol DEPC treated water
Water bath Low-temperature high-speed centrifuge

Move

I. Materials and equipment

1) Phenol: chloroform: isoamyl alcohol (25:24:1).

2) Chloroform: Isoamyl alcohol (2:1)

3) 12mol/L lithium chloride.

4) 3mol/L sodium acetate.

5)70% ethanol.

6)DEPC treated water

7) Water bath.

8) Cryogenic high-speed centrifuge.


II Methods of operation

1) Grind 2~5 g of fungal tissue in a mortar with liquid nitrogen until it is completely powdered.

2) Transfer the ground powder to a Falcon tube containing extraction buffer (3 mL of extraction buffer per gram of fungus) and an equal volume of phenol: chloroform: isoamyl alcohol (preheated to 65°C).

3) Shake the tube to mix thoroughly.

4) Transfer the mixture to an RNase-free centrifuge tube and centrifuge at 13,000~18,000 g for 30 min at 4℃.

5) Collect the upper aqueous phase, add an equal volume of chloroform:isoamyl alcohol (24:1) and mix by turning.

6) Centrifuge at 1300~18000 g for 30 min at 4℃.

7) Collect the upper aqueous phase and add 12mol/L lithium chloride to a final concentration higher than 2mol/L. The final concentration of the aqueous phase was then increased to 2mol/L.

8) Mix and leave at 4°C overnight to precipitate RNA.

9) Centrifuge at 13000~18000 g for 30 min at 4℃.

10) remove the supernatant, wash the precipitate with 5 ml of 3mol/L sodium acetate (pH5.2), and centrifuge for 15 min as in step 9).

11) Remove supernatant. Wash the precipitate with 20 ml of 70% ethanol and centrifuge for 15 min as in step 9).

12) Repeat with 70% ethanol.

13) Vacuum dry to remove ethanol.

14) Dissolve the precipitate in an appropriate volume (250~lOOOul) of DEPC-treated water.

15) Store the dissolved RNA at -70°C.

Caveat

1) When transferring ground fungi into Falcon tubes, do so carefully to avoid loss. All operations should be done quickly and samples/tubes should be kept on ice to minimize the effect of RMase.2) Heat at 65°C to help dissolve the RNA. If there are insoluble particles, centrifuge at 13,000 to 18,000 g for 2 min and collect the supernatant, which contains some or very little RNA or no RNA.


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Categories: Protocols